Deoxycholic acid: bile acid.
Deoxycholic acid testing at Vanguard Laboratory: identity, purity and quantity $250 per sample, with results in 3 to 5 business days.
Deoxycholic acid: 2D structure drawn from the PubChem record (CID 222528).
83-44-3
C24H40O4
392.58 g/mol
Bile acid
Identity: Deoxycholic acid
IUPAC name: (4R)-4-[(3R,5R,8R,9S,10S,12S,13R,14S,17R)-3,12-dihydroxy-10,13-dimethyl-2,3,4,5,6,7,8,9,11,12,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl]pentanoic acid
Method for the $250 identity, purity and quantity test: Chromatographic assay, with detection selected for the compound, against a reference standard, with results in 3 to 5 business days.
The USP monograph covers identity by infrared spectroscopy and HPLC retention time, assay by HPLC, organic impurities by HPLC, lead by atomic absorption, residue on ignition, optical rotation, water, solution clarity and color, bacterial endotoxins and microbial limits. Full testing to the USP Deoxycholic Acid monograph is available and quoted.
Chromatographic purity and mg per unit by the method matched to the compound, identity against a reference standard. 1 unit.
| Add-on test | Price |
|---|---|
| Identity and impurities | |
| FTIR identity | $90 |
| CHNS elemental analysis (carbon, hydrogen, nitrogen, sulfur) | $125 |
| Chiral purity (where a chiral method exists; new methods quoted) | $250 |
| Water, solvents and salt form | |
| Water content by Karl Fischer | $60 |
| Residual solvents | $150 |
| Counterions: chloride, acetate and TFA | $70 |
| Assay | |
| Assay, % w/w (with raw powder purity; $250 together) | +$50 |
| Metals and conformity | |
| Heavy metals: arsenic, cadmium, chromium, mercury and lead | $150 |
| Conformity: purity and quantity on more units from the same lot | $100 per extra unit |
| Microbiology (injectables) | |
| Endotoxin | $210 |
| Sterility or bioburden | $150 |
| Container closure integrity (CCI) | $50 |
| Screening | |
| Fentanyl screen | $50 |
10% off for 10 or more samples.
Need something else? Other tests are available on request.
Purity and quantity is $250 per sample (1 unit) and raw powder purity is $200 for 50 mg, with results in 3 to 5 business days. Send the material sealed and labeled, with the label claim and the form it contains.
No. The $250 test covers identity, purity and quantity by a chromatographic assay, with detection selected for the compound. Full testing to the USP Deoxycholic Acid monograph is available and quoted.
Bile acids have almost no UV chromophore, so the lab uses a detection method suited to the compound.
Other bile acids, such as cholic acid, and isomers of deoxycholic acid are the usual related compounds. Several share a mass with deoxycholic acid, so chromatographic separation matters.
No. They have the same formula, C24H40O4, but the hydroxyl groups sit in different positions. HPLC retention time tells them apart, even though they have the same mass.
https://pubchem.ncbi.nlm.nih.gov/compound/222528
Identity facts from the USP monograph header for this compound.
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