Hibiscus: botanical (flower calyx).
Hibiscus testing at Vanguard Laboratory: identity, purity and quantity $250 per sample, with results in 3 to 5 business days.
Marker compound: 2D structure drawn from the PubChem record (CID 10196837).
Hibiscus sabdariffa Flower
delphinidin 3-sambubioside, cyanidin 3-sambubioside, hibiscus acid
total or named markers, as your specification states
Botanical (flower calyx)
Marker compounds: delphinidin 3-sambubioside, cyanidin 3-sambubioside, hibiscus acid
Method for the $250 identity, purity and quantity test: HPLC-UV marker-compound assay (anthocyanins), LC-MS identity, against a reference standard, with results in 3 to 5 business days.
The USP Herbal Medicines Compendium monograph (proposed for development) covers identity by HPTLC fingerprint and an assay of marker compounds by HPLC.
$250
Chromatographic purity and mg per unit by the method matched to the compound, identity against a reference standard. 1 unit.
| Add-on test | Price |
|---|---|
| Identity and impurities | |
| FTIR identity | $90 |
| CHNS elemental analysis (carbon, hydrogen, nitrogen, sulfur) | $125 |
| Chiral purity (where a chiral method exists; new methods quoted) | $250 |
| Water, solvents and salt form | |
| Water content by Karl Fischer | $60 |
| Residual solvents | $150 |
| Counterions: chloride, acetate and TFA | $70 |
| Assay | |
| Assay, % w/w (with raw powder purity; $250 together) | +$50 |
| Metals and conformity | |
| Heavy metals: arsenic, cadmium, chromium, mercury and lead | $150 |
| Conformity: purity and quantity on more units from the same lot | $100 per extra unit |
10% off for 10 or more samples.
Need something else? Other tests are available on request.
Purity and quantity is $250 per sample (1 unit) and raw powder purity is $200 for 50 mg, with results in 3 to 5 business days. Send the material sealed and labeled, with the label claim and the form it contains.
No. The $250 test covers identity, purity and quantity by HPLC-UV measurement of anthocyanins, with LC-MS identity. The USP Herbal Medicines Compendium monograph for Hibiscus sabdariffa Flower is still in development; testing against it is available and quoted.
The monograph covers the dried calyces and epicalyces, the red fleshy parts around the fruit, not the petals or leaves.
Anthocyanins break down with heat, light and higher pH, so drying and storage affect results. Extracts are prepared under acidic conditions to keep them stable.
https://pubchem.ncbi.nlm.nih.gov/compound/10196837
Identity facts from the USP monograph header for this compound.
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