Job's tears (Coix lacryma-jobi)

Job’s tears: botanical (seed, triglyceride markers).

Job’s tears testing at Vanguard Laboratory: identity, purity and quantity $250 per sample, with results in 3 to 5 business days.

Structure

2D structure of a Job's tears marker compound

Marker compound: 2D structure drawn from the PubChem record (CID 5497163).

Compound data

Botanical source

Coix lacryma-jobi Seed

Marker compounds

triolein, trilinolein, mixed linoleoyl, oleoyl and palmitoyl triglycerides

Basis

total or named markers, as your specification states

Type

Botanical (seed, triglyceride markers)

Structure and names

Marker compounds: triolein (CAS 122-32-7), trilinolein (CAS 537-40-6), mixed linoleoyl, oleoyl and palmitoyl triglycerides

How Vanguard tests Job's tears

Method for the $250 identity, purity and quantity test: Chromatographic marker-compound assay, with detection selected for the compound, against a reference standard, with results in 3 to 5 business days.

The USP Herbal Medicines Compendium monograph covers identity by HPTLC fingerprint and content of seven named triglycerides by HPLC. Full testing to the USP Herbal Medicines Compendium monograph for Coix lacryma-jobi Seed is available and quoted.

What's reported

  • Marker compounds, as % w/w on the basis your specification states
  • Quantity, against the label claim
  • Identity, reported as match or no match against the reference standard
  • With monograph testing (quoted): the monograph’s tests against its limits

Tests and prices

$250

Chromatographic purity and mg per unit by the method matched to the compound, identity against a reference standard. 1 unit.

$200

Chromatographic purity on bulk powder. 50 mg.

Add-on tests

Add-on testPrice
Identity and impurities
FTIR identity$90
CHNS elemental analysis (carbon, hydrogen, nitrogen, sulfur)$125
Chiral purity (where a chiral method exists; new methods quoted)$250
Water, solvents and salt form
Water content by Karl Fischer$60
Residual solvents$150
Counterions: chloride, acetate and TFA$70
Assay
Assay, % w/w (with raw powder purity; $250 together)+$50
Metals and conformity
Heavy metals: arsenic, cadmium, chromium, mercury and lead$150
Conformity: purity and quantity on more units from the same lot$100 per extra unit

10% off for 10 or more samples.

Need something else? Other tests are available on request.

Sample amount and turnaround

Purity and quantity is $250 per sample (1 unit) and raw powder purity is $200 for 50 mg, with results in 3 to 5 business days. Send the material sealed and labeled, with the label claim and the form it contains.

Salts, forms and compendial references

  • Coix lacryma-jobi Seed
  • Coix lacryma-jobi Seed Powder
  • Tell us the salt or form the label states, so quantity is reported on the same basis.

Questions about Job's tears testing

Is the $250 test the same as USP monograph testing?

No. The $250 test covers identity, purity and quantity by a chromatographic assay, with detection selected for the compound. Full testing to the USP Herbal Medicines Compendium monograph for Coix lacryma-jobi Seed is available and quoted.

Why are triglycerides the marker?

Coix seed oil is a characteristic component of the seed, and the monograph sums seven named triglycerides such as triolein and trilinolein.

Does storage affect results?

The seed oil oxidizes once the seed is hulled or ground, which lowers the intact triglycerides. Fresh, cool-stored samples give the most representative result.

Sources

https://pubchem.ncbi.nlm.nih.gov/compound/5497163

Identity facts from the USP monograph header for this compound.

Order

Start an order online, or send the compound name and the tests you need for a quote.