L-asparagine

L-asparagine: amino acid.

L-asparagine testing at Vanguard Laboratory: identity, purity and quantity $250 per sample, with results in 3 to 5 business days.

Structure

L-asparagine: 2D structure drawn from the PubChem record (CID 6267).

Compound data

CAS number

70-47-3

Formula

C₄H₈N₂O₃

Molecular weight

132.12 g/mol

Type

Amino acid

Structure and names

Identity: L-asparagine (anhydrous)

IUPAC name: (2S)-2,4-diamino-4-oxobutanoic acid

How Vanguard tests L-asparagine

Method for the $250 identity, purity and quantity test: Chromatographic assay, with detection selected for the compound, against a reference standard, with results in 3 to 5 business days.

The USP monograph covers identity by infrared spectroscopy and HPLC retention time, assay by HPLC, organic impurities by HPLC, lead, residue on ignition, optical rotation, microbial enumeration, and loss on drying. Full testing to the USP Asparagine monograph is available and quoted.

What's reported

Purity, as percent of total peak area
Quantity, against the label claim
Identity, reported as match or no match against the reference standard
With monograph testing (quoted): the monograph’s tests against its limits

Tests and prices

Purity and quantity

$250

Chromatographic purity and mg per unit by the method matched to the compound, identity against a reference standard. 1 unit.

Raw powder purity

$200

Chromatographic purity on bulk powder. 50 mg.

Add-on tests

Add-on test	Price
Identity and impurities
FTIR identity	$90
CHNS elemental analysis (carbon, hydrogen, nitrogen, sulfur)	$125
Chiral purity (where a chiral method exists; new methods quoted)	$250
Water, solvents and salt form
Water content by Karl Fischer	$60
Residual solvents	$150
Counterions: chloride, acetate and TFA	$70
Assay
Assay, % w/w (with raw powder purity; $250 together)	+$50
Metals and conformity
Heavy metals: arsenic, cadmium, chromium, mercury and lead	$150
Conformity: purity and quantity on more units from the same lot	$100 per extra unit

10% off for 10 or more samples.

Need something else? Other tests are available on request.

Sample amount and turnaround

Purity and quantity is $250 per sample (1 unit) and raw powder purity is $200 for 50 mg, with results in 3 to 5 business days. Send the material sealed and labeled, with the label claim and the form it contains.

Salts, forms and compendial references

Asparagine (anhydrous CAS 70-47-3; monohydrate CAS 5794-13-8)
Tell us the salt or form the label states, so quantity is reported on the same basis.

Questions about L-asparagine testing

Is the $250 test the same as USP monograph testing?

No. The $250 test covers identity, purity and quantity by a chromatographic assay, with detection selected for the compound. Full testing to the USP Asparagine monograph is available and quoted.

Is my asparagine the monohydrate or the anhydrous form?

Asparagine is sold both ways, and the monohydrate carries extra water in its molecular weight. The result is reported on the basis of the labeled form.

Does asparagine degrade?

Asparagine can deamidate to aspartic acid with heat and moisture. The two separate by HPLC and differ in mass by about one dalton.

Sources

https://pubchem.ncbi.nlm.nih.gov/compound/6267

Identity facts from the USP monograph header for this compound.

Order

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